Test Request Details

Environmental and Ecology Test Request


Request: 17-00724

Status: Closed


Description:

UK geology laboratory needed for clay testing for suitability for end uses as clay bricks, tiles, ceramics etc. Scope of testing to include:

Stage 1

An initial gradient firing on each borehole material (10 samples) to determine the firing temperature / colour related to each clay test piece after first milling to a suitable particle size range for clay brick manufacture.

Stage 2 work scope

The following tests will be carried out on the sample as received borehole material (10 samples):

· Particle size distribution - to be determined using both the sedigraph and dry sieving method, to cover the full size range of particles from millimetres to microns. The results would be collated to provide a full particle size distribution.
· XRF Analysis (with Loss on Ignition) - to be carried out to determine the bulk inorganic composition of the following 19 elemental oxides: SiO2, TiO2, CaO, MgO, K2O, Na2O, P2O5, Cr2O3, Mn3O4, ZrO2, HfO2, Al2O3, Fe2, PbO, ZnO, BaO, SrO, SnO2, CuO and SO3 (SO3 reported as remaining after loss on ignition fusion and is not for an accurate SO3 figure).
· Soluble Sulphate using Ion Chromatography on water soluble extract from each borehole.
· Total Carbon & Total Sulphur using the Leco total combustion technique to determine the percentage total sulphur and total carbon of each borehole material.

Stage 3 work scope

The following processing to take place on each borehole material to prepare fired specimens (5 samples selected after stage 2):

· Dried and Fired Shrinkages on five (5) appropriate prepared clay samples: to be tested for each borehole material to determine both the dried shrinkage from green state to after drying at 110 C, and shrinkage from being dried at 110 C to fully fired specimens. The firing temperature will be confirmed for each borehole material after the initial gradient firing.
· Water Absorption - on five (5) appropriate prepared clay samples: to be tested for each fired borehole material
· Summary Report - Summarizing all data with conclusions on the best materials for brick making, referencing typical brick properties.
· Fired samples retained to use as reference samples


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