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Laboratory Test Request Details

Test Request


Request: 15-01718

Status: Closed


Description:

Materials Laboratory needed for required Filter Testing (Directly from US Code of Federal Regulators, 40 CFR Part 50 Appendix L,Reference Method for the Determination of Fine Particulate Matter as PM2.5 in the Atmosphere )

6.5 Filter thickness. 30 to 50 µm.

6.6 Maximum pressure drop (clean filter). 30 cm H2O column @ 16.67 L/min clean air flow.
6.7 Maximum moisture pickup. Not more than 10 µg weight increase after 24-hour exposure to air of 40 percent relative humidity, relative to weight after 24-hour exposure to air of 35 percent relative humidity.
6.8 Collection efficiency. Greater than 99.7 percent, as measured by the DOP test (ASTM D 2986-91) with 0.3 µm particles at the sampler's operating face velocity.
6.9 Filter weight stability. Filter weight loss shall be less than 20 µg, as measured in each of the following two tests specified in sections 6.9.1 and 6.9.2 of this appendix. The following conditions apply to both of these tests: Filter weight loss shall be the average difference between the initial and the final filter weights of a random sample of test filters selected from each lot prior to sale. The number of filters tested shall be not less than 0.1 percent of the filters of each manufacturing lot, or 10 filters, whichever is greater. The filters shall be weighed under laboratory conditions and shall have had no air sample passed through them, i.e., filter blanks. Each test procedure must include initial conditioning and weighing, the test, and final conditioning and weighing. Conditioning and weighing shall be in accordance with sections 8.0 through 8.2 of this appendix and general guidance provided in reference 2 of section 13.0 of this appendix.
6.9.1 Test for loose, surface particle contamination. After the initial weighing, install each test filter, in turn, in a filter cassette (Figures L-27, L-28, and L-29 of this appendix) and drop the cassette from a height of 25 cm to a flat hard surface, such as a particle-free wood bench. Repeat two times, for a total of three drop tests for each test filter. Remove the test filter from the cassette and weigh the filter. The average change in weight must be less than 20 µg.
6.9.2 Test for temperature stability. After weighing each filter, place the test filters in a drying oven set at 40 °C ±2 °C for not less than 48 hours. Remove, condition, and reweigh each test filter. The average change in weight must be less than 20 µg.
6.10 Alkalinity. Less than 25 microequivalents/gram of filter, as measured by the guidance given in reference 2 in section 13.0 of this appendix.
6.11 Supplemental requirements. Although not required for determination of PM2.5 mass concentration under this reference method, additional specifications for the filter must be developed by users who intend to subject PM2.5 filter samples to subsequent chemical analysis. These supplemental specifications include background chemical contamination of the filter and any other filter parameters that may be required by the method of chemical analysis. All such supplemental filter specifications must be compatible with and secondary to the primary filter specifications given in this section 6.0 of this appendix.


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